Practical Inductively Coupled Plasma Spectrometry
Autor John R. Deanen Limba Engleză Hardback – 4 iun 2019
The second edition of Practical Inductively Coupled Plasma Spectrometry discusses many of the significant developments in the field which have expanded inductively coupled plasma (ICP) spectrometry from a useful optical emission spectroscopic technique for trace element analysis into a source for both atomic emission spectrometry and mass spectrometry, capable of detecting elements at sub-ppb (ng mL-1) levels with good accuracy and precision.
Comprising nine chapters, this new edition has been fully revised and updated in each chapter. It contains information on everything you need to practically know about the different types of instrumentation as well as pre- and post-experimental aspects. Designed to be easily accessible, with a 'start-to-finish' approach, each chapter outlines the key practical aspects of a specific aspect of the topic. The author, a noted expert in the field, details specific applications of the techniques presented, including uses in environmental, food and industrial analysis.
This edition:
- Emphasizes the importance of health and safety;
- Provides advanced information on sample preparation techniques;
- Presents an updated chapter on inductively coupled plasma mass spectrometry;
- Features a new chapter on current and future development in ICP technology and one on practical trouble shooting and routine maintenance.
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Specificații
ISBN-13: 9781119478683
ISBN-10: 1119478685
Pagini: 248
Dimensiuni: 156 x 233 x 17 mm
Greutate: 0.53 kg
Ediția:2nd edition
Editura: Wiley
Locul publicării:Chichester, United Kingdom
ISBN-10: 1119478685
Pagini: 248
Dimensiuni: 156 x 233 x 17 mm
Greutate: 0.53 kg
Ediția:2nd edition
Editura: Wiley
Locul publicării:Chichester, United Kingdom
Notă biografică
John R. Dean is Professor of Analytical and Environmental Sciences and Head of Subject (Analytical Sciences), in the Department of Applied Sciences, at Northumbria University where he has worked since 1988. He is a Chartered Scientist, Chartered Chemist, Fellow of the Royal Society of Chemistry and Principal Fellow of the Higher Education Academy. His broad and varied research interests include chemical measurement of potentially harmful elements, persistent organic pollutants and nanomaterials in environmental matrices to assess their human health risk assessment as well as analysis of volatile compounds from pathogenic bacteria for disease identification.
Cuprins
About the Author xiii
Preface xv
Acknowledgements xix
Acronyms, Abbreviations and Symbols xxiii
1 The Analytical Approach 1
1.1 Introduction 1
1.2 Essentials of Practical Work 2
1.3 Health and Safety 3
1.4 SI Units and Their Use 4
1.5 Significant Figures 11
1.6 Calibration and Quantitative Analysis 12
1.7 Making Notes of Practical Work and Observations 13
1.8 Data Analysis 14
1.9 Data Treatment 17
1.10 Data Quality 18
1.11 Data Interpretation and Context 21
1.12 Analytical Terms and Their Definitions 21
1.13 Summary 26
2 Sampling and Storage 27
2.1 Introduction 27
2.2 Sampling Soil 28
2.3 Sampling Water 31
2.4 Sampling Air 32
2.5 Sample Storage 34
2.6 Sample Preservation 36
2.7 Summary 37
3 Sample Preparation 39
3.1 Introduction 39
3.2 Aqueous Samples 40
3.3 Solid Samples 43
3.4 Extraction Procedures 51
3.5 Summary 69
4 Sample Introduction 75
4.1 Introduction 75
4.2 Nebulizers 76
4.3 Spray Chambers and Desolvation Systems 79
4.4 Discrete Sample Introduction 83
4.5 Continuous Sample Introduction 87
4.6 Hydride and Cold-Vapour Generation Techniques 91
4.7 Summary 93
5 The Inductively Coupled Plasma 95
5.1 Introduction 95
5.2 Radiofrequency Generators 96
5.3 Inductively Coupled Plasma Formation and Operation 96
5.4 Processes Within the ICP 106
5.5 Signal Processing and Instrument Control 106
5.6 Summary 107
6 Inductively Coupled Plasma-Atomic Emission Spectrometry 109
6.1 Introduction 110
6.2 Fundamentals of Spectroscopy 110
6.3 Plasma Spectroscopy 116
6.4 Spectrometers 118
6.5 Detectors 125
6.6 Interferences 130
6.7 Summary 131
7 Inductively Coupled Plasma-Mass Spectrometry 133
7.1 Introduction 133
7.2 Fundamentals of Mass Spectrometry 134
7.3 Inorganic Mass Spectrometry 135
7.4 Mass Spectrometers 139
7.5 Detectors 153
7.6 Interferences 156
7.7 Isotope Dilution Analysis 165
7.8 Summary 176
8 Inductively Coupled Plasma: Current and Future Developments 177
8.1 Introduction 177
8.2 Comparison of ICP-AES and ICP-MS 177
8.3 Applications 182
8.4 Current and Future Developments 183
8.5 Useful Resources 191
9 Inductively Coupled Plasma: Troubleshooting and Maintenance 201
9.1 Introduction 201
9.2 Diagnostic Issues 201
9.3 Tips to Reduce... 202
9.4 Tips to Improve... 203
9.5 How To... 203
9.6 What to do About... 204
9.7 Shut Down Procedure (At the End of the Day) 204
9.8 Regular Maintenance Schedule 205
The Periodic Table 207
SI Units and Physical Constants 209
Index 213
Preface xv
Acknowledgements xix
Acronyms, Abbreviations and Symbols xxiii
1 The Analytical Approach 1
1.1 Introduction 1
1.2 Essentials of Practical Work 2
1.3 Health and Safety 3
1.4 SI Units and Their Use 4
1.5 Significant Figures 11
1.6 Calibration and Quantitative Analysis 12
1.7 Making Notes of Practical Work and Observations 13
1.8 Data Analysis 14
1.9 Data Treatment 17
1.10 Data Quality 18
1.11 Data Interpretation and Context 21
1.12 Analytical Terms and Their Definitions 21
1.13 Summary 26
2 Sampling and Storage 27
2.1 Introduction 27
2.2 Sampling Soil 28
2.3 Sampling Water 31
2.4 Sampling Air 32
2.5 Sample Storage 34
2.6 Sample Preservation 36
2.7 Summary 37
3 Sample Preparation 39
3.1 Introduction 39
3.2 Aqueous Samples 40
3.3 Solid Samples 43
3.4 Extraction Procedures 51
3.5 Summary 69
4 Sample Introduction 75
4.1 Introduction 75
4.2 Nebulizers 76
4.3 Spray Chambers and Desolvation Systems 79
4.4 Discrete Sample Introduction 83
4.5 Continuous Sample Introduction 87
4.6 Hydride and Cold-Vapour Generation Techniques 91
4.7 Summary 93
5 The Inductively Coupled Plasma 95
5.1 Introduction 95
5.2 Radiofrequency Generators 96
5.3 Inductively Coupled Plasma Formation and Operation 96
5.4 Processes Within the ICP 106
5.5 Signal Processing and Instrument Control 106
5.6 Summary 107
6 Inductively Coupled Plasma-Atomic Emission Spectrometry 109
6.1 Introduction 110
6.2 Fundamentals of Spectroscopy 110
6.3 Plasma Spectroscopy 116
6.4 Spectrometers 118
6.5 Detectors 125
6.6 Interferences 130
6.7 Summary 131
7 Inductively Coupled Plasma-Mass Spectrometry 133
7.1 Introduction 133
7.2 Fundamentals of Mass Spectrometry 134
7.3 Inorganic Mass Spectrometry 135
7.4 Mass Spectrometers 139
7.5 Detectors 153
7.6 Interferences 156
7.7 Isotope Dilution Analysis 165
7.8 Summary 176
8 Inductively Coupled Plasma: Current and Future Developments 177
8.1 Introduction 177
8.2 Comparison of ICP-AES and ICP-MS 177
8.3 Applications 182
8.4 Current and Future Developments 183
8.5 Useful Resources 191
9 Inductively Coupled Plasma: Troubleshooting and Maintenance 201
9.1 Introduction 201
9.2 Diagnostic Issues 201
9.3 Tips to Reduce... 202
9.4 Tips to Improve... 203
9.5 How To... 203
9.6 What to do About... 204
9.7 Shut Down Procedure (At the End of the Day) 204
9.8 Regular Maintenance Schedule 205
The Periodic Table 207
SI Units and Physical Constants 209
Index 213