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Practical Organic Chemistry: A student handbook of techniques

Editat de J.T. Sharp
en Limba Engleză Paperback – 26 ian 1989
One of the very best things about organic chemistry is actually doing experimental work at the beneh. This applies not only at the profes­ sionallevel but also from the earliest stages of apprenticeship to the craft as a student. The fascination sterns from the nature of the sub­ ject itself, with its vast array of different types of reaction and its al­ most infinite variety of different chemical compounds. Each reaction and each new compound pose their own particular problems to chal­ lenge the skill and ingenuity of the chemist, whether working in a first-year teaching la bora tory or at the frontiers of research. This book is intended to provide basic guidance in the essential experimental techniques used in a typical undergraduate course. It gives concise coverage of the range of practical skills required, from first-year level when students may have no previous experience, up to final-year level when students are usually involved in more complex and dem an ding experimental workin supervised research projects. Our objective was to produce a handbook of techniques that could be used with a variety of practical courses throughout a student's whole period of study. Those who run practical courses generally have strong feelings about what particular experiments or exercises are appropriate for their own students, and it is rare that a book of experiments suitable for one department is acceptable to another.
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Specificații

ISBN-13: 9780412282300
ISBN-10: 0412282305
Pagini: 200
Ilustrații: XVI, 200 p.
Dimensiuni: 155 x 235 x 13 mm
Greutate: 0.31 kg
Editura: SPRINGER NETHERLANDS
Colecția Springer
Locul publicării:Dordrecht, Netherlands

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Cuprins

1 Introduction.- 1.1 The range of experimental techniques.- 1.2 Good laboratory practice.- 1.3 Safety in the laboratory.- 1.4 Keeping records.- 1.5 Samples and spectra.- 2 Carrying out reactions.- 2.1 Basic techniques.- 2.2 Special techniques.- 3 Isolation and purification of reaction products.- 3.1 Primary work-up procedures.- 3.2 Crystallization.- 3.3 Melting point.- 3.4 Distillation.- 4 Separation of organic mixtures by chromatography.- 4.1 Analytical methods.- 4.2 Preparative methods.- 4.3 Appendices.- Preparation of samples for spectroscopy.- 5.1 Infra-red.- 5.2 Nuclear magnetic resonance.- 5.3 Mass spectrometry.- 5.4 Ultraviolet.- Finding chemical information.- 6.1 Physical properties.- 6.2 Spectroscopic properties.- 6.3 Beilstein’s Handbuch.- 6.4 Chemical Abstracts.