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Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers

Autor John S. Harwood, Huaping Mo
en Limba Engleză Paperback – 27 oct 2015
Practical NMR Spectroscopy Laboratory Guide is designed to provide non-expert NMR users, typically graduate students in chemistry, an introduction to various facets of practical solution-state NMR spectroscopy. Each chapter offers a series of hands-on exercises, introducing various NMR concepts and experiments and guiding the reader in running these experiments using an NMR spectrometer. The book is written for use with a Bruker NMR spectrometer running TopSpin software versions 1 or 2. This practical resource functions both as a text for instructors of a practical NMR course and also as a reference for spectrometer administrators or NMR facility directors when doing user training. This guide serves as serve as excellent, practical resource on its own or as a companion book to Timothy Claridge’s High-Resolution NMR Techniques in Organic Chemistry, 2nd Edition (Elsevier, 2009).

  • Written by experts in solution-state NMR spectroscopy
  • Provides step-by-step instructions for more than 50 activities using a Bruker NMR spectrometer
  • Includes detailed appendices and sample questions for lab reports
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Specificații

ISBN-13: 9780128006894
ISBN-10: 0128006897
Pagini: 136
Ilustrații: 40 illustrations
Dimensiuni: 152 x 229 x 8 mm
Greutate: 0.2 kg
Editura: ELSEVIER SCIENCE

Public țintă

Graduate students in chemistry and related disciplines taking courses in NMR spectroscopy

Cuprins

Introduction1. Basics and Spectrometer Performance Checks2. Multiple Irradiation and Multiple Pulse Experiments3. Polarization Transfer and Its Applications4. Homonuclear Correlation Experiments5. PFG (Pulsed Field Gradient) Experiments6. Introduction to NMR of Biomolecules in H2O7. Selective Experiments Using Shaped Pulses8. Diffusion Measurements and DOSY (Diffusion Ordered SpectroscopY)

Notă biografică

Dr. John Simon Harwood has served as Director of the Purdue University Interdepartmental NMR Facility (PINMRF) since 2005, where he has overseen the rationalization and expansion of PINMRF such that the facility now includes two spectrometers with cryoprobes along with an 800-MHz spectrometer. He holds a DSc in Chemistry from the University of Texas at Arlington, and he's held postdoctoral positions at University of Texas Southwestern Medical School and University of California, Berkeley. He is a former manager of the NMR Facility in the Chemistry Department, University of Georgia, and a former director of both the NMR Facilities and the Computational Facility in the Chemistry Department, University of Illinois, Chicago.