Modern Glass Characterization
Editat de Mario Affatigatoen Limba Engleză Hardback – 5 oct 2015
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Specificații
ISBN-13: 9781118230862
ISBN-10: 1118230868
Pagini: 464
Dimensiuni: 161 x 244 x 32 mm
Greutate: 0.8 kg
Editura: JOHN WILEY & SONS INC
Locul publicării:Hoboken, United States
ISBN-10: 1118230868
Pagini: 464
Dimensiuni: 161 x 244 x 32 mm
Greutate: 0.8 kg
Editura: JOHN WILEY & SONS INC
Locul publicării:Hoboken, United States
Public țintă
Researchers, graduates, experts in the field of glass science and closely related areas (e.g. materials scientists who use glass as a primary component in their work), including those in both academia and industryNotă biografică
Mario Affatigato, PhD,is currently Professor of Physics at Coe College, Iowa. Prof. Affatigato's research interests include optical properties of glasses and the relationship between those properties and the structure of the glass. He was awarded the Presidential Early Career Award for Scientists and Engineers in 1999, and the Faculty Member Prize for Research in an Undergraduate Institution in 2013 by the American Physical Society. He has published over 80 papers in refereed journals.
Cuprins
Preface xiii
List of Contributors xv
1 DENSITY, THERMAL PROPERTIES, AND THE GLASS TRANSITION TEMPERATURE OF GLASSES 1
Steve Feller
Part I: Introduction to Physical Properties and Their Uses 1
Part II: Density 2
1.1 Density: Experimental Background and Theory 2
Part III: Thermal Effects with a Focus on the Glass Transition Temperature 20
1.2 OVERVIEW 20
1.3 EXPERIMENTAL METHODS AND THEORY 20
1.4 INSTRUMENTATION USED FOR DETERMINING Tg AND RELATED THERMAL EVENTS 23
1.5 ANALYSIS OF DATA AND EXTRACTION OF USEFUL INFORMATION 25
1.6 CASE STUDIES FROM GLASS SYSTEMS 26
1.7 CONCLUSION TO THERMAL PROPERTIES 30
2 INFRARED SPECTROSCOPY OF GLASSES 32
E.I. Kamitsos
2.1 INTRODUCTION 32
2.2 BACKGROUND AND THEORY 34
2.3 INSTRUMENTATION 44
2.4 ANALYSIS OF INFRARED DATA 48
2.6 CONCLUSIONS 68
3 RAMAN SPECTROSCOPY OF GLASSES 74
Rui M. Almeida and Luis F. Santos
3.1 INTRODUCTION 74
3.2 BACKGROUND 76
3.3 INSTRUMENTATION AND DATA ANALYSIS 80
3.4 CASE STUDIES 87
3.5 CONCLUSIONS 103
4 BRILLOUIN LIGHT SCATTERING 107
John Kieffer
4.1 INTRODUCTION 107
4.2 BACKGROUND AND THEORY 110
4.3 INSTRUMENTATION 117
4.4 DATA ANALYSIS AND INFORMATION CONTENT 126
4.5 EXAMPLES OF CASE STUDIES 133
4.6 SUMMARY 154
5 NEUTRON DIFFRACTION TECHNIQUES FOR STRUCTURAL STUDIES OF GLASSES 158
Alex C. Hannon
5.1 INTRODUCTION 158
5.2 INSTRUMENTATION 159
5.3 THEORETICAL ASPECTS OF NEUTRON DIFFRACTION ON GLASSES 169
5.4 THE APPLICATION OF NEUTRON DIFFRACTION TO STUDIES OF GLASS STRUCTURE 186
6 X-RAY DIFFRACTION FROM GLASS 241
Christopher J. Benmore
6.1 INTRODUCTION 241
6.2 BACKGROUND/THEORY 244
6.3 ANALYSIS OF DATA, EXTRACTION OF USEFUL INFORMATION 249
6.4 INSTRUMENTATION 255
6.5 CASE STUDIES 258
6.6 CONCLUSIONS 264
7 XAFS SPECTROSCOPY AND GLASS STRUCTURE 271
Giuseppe Dalba and Francesco Rocca
7.1 INTRODUCTION 271
7.2 THE ORIGINS OF X-RAY ABSORPTION SPECTRA 272
7.3 XAFS INSTRUMENTATION 274
7.4 THE PHYSICAL MECHANISM OF XAFS 278
7.5 EXAFS 279
7.6 XAFS DATA ANALYSIS 284
7.7 EXAFS ACCURACY AND LIMITATIONS 289
7.8 XANES 290
7.9 XAFS SPECTROSCOPY APPLIED TO GLASS STRUCTURE: SOME EXAMPLES 291
7.10 SUMMARY AND CONCLUSIONS 309
8 NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY OF GLASSES 315
Scott Kroeker
8.1 INTRODUCTION 315
8.2 THEORETICAL BACKGROUND 316
8.3 INSTRUMENTATION 323
8.4 DATA ANALYSIS AND STRUCTURAL INTERPRETATION 329
8.5 CASE STUDIES 333
8.6 CONCLUSIONS 341
9 ADVANCED DIPOLAR SOLID STATE NMR SPECTROSCOPY OF GLASSES 345
Hellmut Eckert
9.1 INTRODUCTION 345
9.2 THEORETICAL ASPECTS 347
9.3 HETERONUCLEAR EXPERIMENTS 349
9.4 HOMONUCLEAR EXPERIMENTS 360
9.5 CASE STUDIES 370
10 ATOM PROBE TOMOGRAPHY OF GLASSES 391
Daniel Schreiber and Joseph V. Ryan
10.1 INTRODUCTION 391
10.2 BACKGROUND AND THEORY 392
10.3 INSTRUMENTATION 395
10.4 ANALYSIS METHODS 409
10.5 CASE STUDIES 417
Index 431
1 DENSITY, THERMAL PROPERTIES, AND THE GLASS TRANSITION TEMPERATURE OF GLASSES 1
Steve Feller
Part I: Introduction to Physical Properties and Their Uses 1
Part II: Density 2
1.1 Density: Experimental Background and Theory 2
Part III: Thermal Effects with a Focus on the Glass Transition Temperature 20
1.2 OVERVIEW 20
1.3 EXPERIMENTAL METHODS AND THEORY 20
1.4 INSTRUMENTATION USED FOR DETERMINING Tg AND RELATED THERMAL EVENTS 23
1.5 ANALYSIS OF DATA AND EXTRACTION OF USEFUL INFORMATION 25
1.6 CASE STUDIES FROM GLASS SYSTEMS 26
1.7 CONCLUSION TO THERMAL PROPERTIES 30
2 INFRARED SPECTROSCOPY OF GLASSES 32
E.I. Kamitsos
2.1 INTRODUCTION 32
2.2 BACKGROUND AND THEORY 34
2.3 INSTRUMENTATION 44
2.4 ANALYSIS OF INFRARED DATA 48
2.6 CONCLUSIONS 68
3 RAMAN SPECTROSCOPY OF GLASSES 74
Rui M. Almeida and Luis F. Santos
3.1 INTRODUCTION 74
3.2 BACKGROUND 76
3.3 INSTRUMENTATION AND DATA ANALYSIS 80
3.4 CASE STUDIES 87
3.5 CONCLUSIONS 103
4 BRILLOUIN LIGHT SCATTERING 107
John Kieffer
4.1 INTRODUCTION 107
4.2 BACKGROUND AND THEORY 110
4.3 INSTRUMENTATION 117
4.4 DATA ANALYSIS AND INFORMATION CONTENT 126
4.5 EXAMPLES OF CASE STUDIES 133
4.6 SUMMARY 154
5 NEUTRON DIFFRACTION TECHNIQUES FOR STRUCTURAL STUDIES OF GLASSES 158
Alex C. Hannon
5.1 INTRODUCTION 158
5.2 INSTRUMENTATION 159
5.3 THEORETICAL ASPECTS OF NEUTRON DIFFRACTION ON GLASSES 169
5.4 THE APPLICATION OF NEUTRON DIFFRACTION TO STUDIES OF GLASS STRUCTURE 186
6 X-RAY DIFFRACTION FROM GLASS 241
Christopher J. Benmore
6.1 INTRODUCTION 241
6.2 BACKGROUND/THEORY 244
6.3 ANALYSIS OF DATA, EXTRACTION OF USEFUL INFORMATION 249
6.4 INSTRUMENTATION 255
6.5 CASE STUDIES 258
6.6 CONCLUSIONS 264
7 XAFS SPECTROSCOPY AND GLASS STRUCTURE 271
Giuseppe Dalba and Francesco Rocca
7.1 INTRODUCTION 271
7.2 THE ORIGINS OF X-RAY ABSORPTION SPECTRA 272
7.3 XAFS INSTRUMENTATION 274
7.4 THE PHYSICAL MECHANISM OF XAFS 278
7.5 EXAFS 279
7.6 XAFS DATA ANALYSIS 284
7.7 EXAFS ACCURACY AND LIMITATIONS 289
7.8 XANES 290
7.9 XAFS SPECTROSCOPY APPLIED TO GLASS STRUCTURE: SOME EXAMPLES 291
7.10 SUMMARY AND CONCLUSIONS 309
8 NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY OF GLASSES 315
Scott Kroeker
8.1 INTRODUCTION 315
8.2 THEORETICAL BACKGROUND 316
8.3 INSTRUMENTATION 323
8.4 DATA ANALYSIS AND STRUCTURAL INTERPRETATION 329
8.5 CASE STUDIES 333
8.6 CONCLUSIONS 341
9 ADVANCED DIPOLAR SOLID STATE NMR SPECTROSCOPY OF GLASSES 345
Hellmut Eckert
9.1 INTRODUCTION 345
9.2 THEORETICAL ASPECTS 347
9.3 HETERONUCLEAR EXPERIMENTS 349
9.4 HOMONUCLEAR EXPERIMENTS 360
9.5 CASE STUDIES 370
10 ATOM PROBE TOMOGRAPHY OF GLASSES 391
Daniel Schreiber and Joseph V. Ryan
10.1 INTRODUCTION 391
10.2 BACKGROUND AND THEORY 392
10.3 INSTRUMENTATION 395
10.4 ANALYSIS METHODS 409
10.5 CASE STUDIES 417
Index 431
Descriere
The book consists of a series of edited chapters, each written by an expert in the field and focusing on a particular characterization technique as applied to glass.