Water is an essential resource for living systems, industrial processes, agricultural production and domestic use. It is one of the most precious gift of nature without which no life could survive on earth. In the recent past several studies have reported the water bodies becoming increasingly contaminated due to domestic and industrial waste. Water pollution affects our oceans, lakes, rivers, and drinking water, making it a widespread and global concern. This research focuses on synthesis of natural polymer based new resins and fly ash based zeolites for developing a cost effective technology for treatment of heavy metals, contaminated industrial waste water. Main toxic hazardous metal ions present in the various effluents are Fe, Cu, Pb, Al, Cr, Cd, Zn, Ni etc. Fly ash is byproduct of thermal power plants. This ash is waste for them so it is easily available & economy. Synthesis of zeolites from fly ash is a better way for utilization of waste fly ash for the effluent treatment.