Analytical chemistry is a branch of chemistry that determines the nature and identity of a substance and its composition. Analytical methods are ability to provide timely, accurate, and reliable data is central to the discovery, development, and manufacture of pharmaceuticals. The developed assay method was found to be simple, accurate, sensitive, précised, specific and rapid. This method can be applied for routine quantitative analysis of Paracetamol and Lornoxicam in pharmaceutical formulations like Tablet dosage form.